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QuickTOC analyser for TOC/COD in cheese production

A Metrohm (UK) product story
Edited by the Processingtalk editorial team Jun 11, 2009

Cheese producers are looking for a reliable COD measurement to optimise the production of cheese and reduce the surcharges in wastewater treatment.

The idea is to separate the high-strength waste from the low-strength waste.

The low-strength waste could be sent directly to the sewer without treatment.

The high-strength waste could be diverted, separated and the milk products recovered for re-use in production.

This idea would potentially save thousands of pounds in sewage surcharges and yield more products from the same amount of milk.

There are several things in this process that makes this a difficult measurement.

The untreated wastewater in cheese production has very high concentrations of salt, milk fat, raw milk and high levels of suspended solids.

In addition, the waste stream also has a pH that varies form 4pH to 12pH due to the clean-in-place (CIP) processes.

To make this idea pay off, there would have to be a reliable/repeatable system with minimal maintenance.

It has been determined that a correlation could be made between COD and TOC in this application.

It is also possible to use TOC to monitor CBOD (carbonatious biological oxygen demand).

The only way to perform the correlation in this application is high-temperature combustion in a range of 100-10,000 mg/l TOC.

The LAR QuickTOC is chosen for a number of reasons.

Because of the high concentrations of salt in the process, a system with a large reaction chamber and very high temperature was needed.

The LAR reaction chamber is very large, and this, coupled with the 1,200C furnace, made it an ideal choice.

At 1,200C sodium chloride (salt) passes through the reaction chamber reducing the maintenance time required.

The second reason is the high concentration of suspended solids in the sample.

The QuickTOC, using the LAR flow sampler, can handle high-concentration suspended solids in a waste stream without pre-filtration.

This, in conjunction with the large bore tubing used for sample transfer and an innovative method of delivering the sample into the reaction chamber, proves to be a low maintenance and reliable method.

Find out more about this article. Request a brochure, download technical specifications and request samples here.

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